Acta Univ. Agric. Silvic. Mendelianae Brun. 2011, 59(1), 255-262 | DOI: 10.11118/actaun201159010255
The changes of flavour and aroma active compounds content during production of Edam cheese
- Ústav chemie potravin a biotechnologií, Vysoké učení technické v Brně, Purkyňova 118, 612 00 Brno, Česká republika
This work deals with the problem of flavour of Edam cheeses, i.e. natural hard cheese with low heat curd. The cheese samples were produced in dairy MILTRA B, Ltd., Městečko Trnávka.
A number of volatile substances contribute to flavour of cheese including alcohols, aldehydes, ketones, fatty acids, esters, lactones, terpenes etc. The development of these components during production was monitored in chosen Edam cheese (fat 30% w/w) using headspace-SPME-GC method. The samples were taken from cheesemilk up to technologically ripe cheese. In total 37 various organic compounds belonging to five chemical groups were identified in milk and cheese samples. Their total content increased during production. The first increase was observed after pressing and then especially in last part of ripening. Ethanol (185.8 ± 15.85 mg.kg-1), acetoin (97.7 ± 3.78 mg.kg-1), 2-methylpropanol (71.2 ± 5.23 mg.kg-1), acetic acid (54.4 ± 1.70 mg.kg-1) and acetaldehyde (36.4 ± 10.17 mg.kg-1) were the most abundant in ripened cheeses.
The flavour and other organoleptic properties (appearance, texture) of Edam cheese samples were also sensorially evaluated during ripening. The five point ordinal scale and profile tests were used for evaluation. The sensory quality was improved during ripening, until the final marked flavour characteristic for these cheese types.
Keywords: Edam cheese, flavour, aroma active compounds, GC, SPME, sensory analysis
Grants and funding:
This work was kindly supported by a project of Ministry of Education, Youth and Sports of the Czech Republic (Grant No. MSM 0021630501).
Received: October 20, 2010; Published: July 10, 2014 Show citation
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References
- ALEWIJN, M., SLIWINSKI, E. L., WOUTERS, J. T. M., 2005: Production of fat-derived (flavour) compounds during the ripening of Gouda cheese. International Dairy Journal, 15, 6-9: 733-740. ISSN: 0958-6946. DOI: 10.1016/j.idairyj.2004.09.009
Go to original source...
- CURIONI, P. M. G., BOSSET, J. O., 2002: Key odorants in various cheese types as determined by gas chromatography-olfactometry. International Dairy Journal, 12, 12: 959-984. ISSN: 0958-6946. DOI: 10.1016/S0958-6946(02)00124-3
Go to original source...
- FOX, P. F., GUINEE, T. P., COGAN, T. M., McSWEENEY, P. L. H., 2000: Fundamentals of Cheese Science. 1st. ed. Gauthersburg (Maryland, USA): Aspen Publication, 638 p. ISBN 0-8342-1260-9.
- ISO 6564:1985. Sensory analysis-Methodology-Flavour profile methods. International Organization for Standardization, Geneva, Switzerland, 1985, 6 p.
- ISO 8589:2007. Sensory analysis-General guidance for the design of test rooms. International Organization for Standardization, Geneva, Switzerland, 2007, 2. ed., 16 p.
- KRAGGERUD, H., SKEIE, S., HOY, M., ROKKE, L., ABRAHAMSEN, R. K., 2008: Season and ripening temperature influence fatty acid composition and sensory properties of semi-hard cheese during maturation. International Dairy Journal, 18, 8: 801-810. ISSN: 0958-6946. DOI: 10.1016/j.idairyj.2007.11.003
Go to original source...
- KUCUKONER, E., HAQUE, Z. U., 2003: Physico-chemical and rheological properties of full fat and low fat Edam cheeses. European Food Research and Technology, 217, 4: 281-286. ISSN: 1438-2377. DOI: 10.1007/s00217-003-0752-x
Go to original source...
- LECANU, L., DUCRUET, V., JOUQUAND, C., GRATADOUX, J. J., FEIGENBAUM, A., 2002: Optimization of headspace solid-phase microextraction (SPME) for the odor analysis of surface-ripened cheese. Journal of Agricultural and Food Chemistry, 50, 13: 3810-3817. ISSN: 0021-8561. DOI: 10.1021/jf0117107
Go to original source...
- LUŽOVÁ, T., POVOLNÁ, Š., NEDOMOVÁ, Š., ŠUSTOVÁ, K., BLAŠKOVÁ, V., 2008: Influence of ripening of Edam cheese on texture properties. Acta universitatis agriculturae et silviculturae Mendelianae Brunensis, 56, 2: 107-114. ISSN: 1211-8516. DOI: 10.11118/actaun200856020107
Go to original source...
- McSWEENEY, P. L. H., SOUSA, M. J., 2000: Biochemical pathways for the production of flavour compounds in cheese during ripening: A review. Lait, 80, 3: 293-324. ISSN: 0023-7302. DOI: 10.1051/lait:2000127
Go to original source...
- McSWEENEY, P. L. H., 2004: Biochemistry of cheese ripening. International Journal of Dairy Technology, 57, 2-3: 127-144. ISSN: 1364-727X. DOI: 10.1111/j.1471-0307.2004.00147.x
Go to original source...
- McSWEENEY, P. L. H., HAYALOGLU, A. A., O'MAHONY, J. A., BANSAL, N., 2006: Perspectives on cheese ripening. Australian Journal of Dairy Technology, 61, 2: 69-77. ISSN: 0004-9433.
- MONDELLO, L., COSTA, R., TRANCHIDA, P. Q., CHIOFALO, B., ZUMBO, A., DUGO, P., DUGO, G., 2005. Determination of flavor components in Sicilian goat cheese by automated HS-SPME-GC. Flavour and Fragrance Journal, 20, 6: 659-665. ISSN: 0882-5734. DOI: 10.1002/ffj.1529
Go to original source...
- NEDOMOVÁ, Š., 2010: Viscoelasticity of Edam cheese during its ripening. Acta universitatis agriculturae et silviculturae Mendelianae Brunensis, 58, 4: 183-192. ISSN: 1211-8516. DOI: 10.11118/actaun201058040183
Go to original source...
- NHUCH, E. L., PRIETO, B., FRANCO, I., BERNANDO, A., CARBALLO, J., 2008: Biochemical changes during the ripening of San Simón da Costa cheese (PDO) manufactured from pasteurised milk. Australian Journal of Dairy Technology, 63, 2: 68-76. ISSN: 0004-9433.
Go to original source...
- PACHLOVÁ, V., BUŇKA, F., BUŇKOVÁ, L., WEISEROVÁ, E., HLADKÁ, K., VOJTÍŠKOVÁ, P., KRÁČMAR, S., 2009: Vliv průběhu zrání na obsah vybraných složek v přírodním sýru eidamského typu. Potravinárstvo, 3, 1: 33-36. ISSN: 1337-0960.
- PINHO, O., FERREIRA, I. M. P. L. V. O., FERREIRA, M. A., 2002: Solid-phase microextraction in combination with GC/MS for quantification of the major volatile free fatty acids in ewe cheese. Analytical chemistry, 74, 20: 5199-5204. ISSN: 0003-2700. DOI: 10.1021/ac020296m
Go to original source...
- REHMAN, S. U., BANKS, J. M., BRECHANY, E. Y., MUIR, D. D., MCSWEENEY, P. L. H., FOX, P. F., 2000: Influence of ripening temperature on the volatiles profile and flavour of Cheddar cheese made from raw or pasteurised milk. International Dairy Journal, 10, 1-2: 55-65. ISSN: 0958-6946. DOI: 10.1016/S0958-6946(00)00019-4
Go to original source...
- RITVANEN, T., LAMPOLAHTI, S., LILLEBERG, L., TUPASELA, T., ISONIEMI, M., APPELBYE, U., LYYTIKAINEN, T., EEROLA, S., UUSI-RAUVA, E., 2005: Sensory evaluation, chemical composition and consumer acceptance of full fat and reduced fat cheeses in the Finnish market. Food Quality and Preference, 16, 6: 479-492. ISSN: 0950-3293. DOI: 10.1016/j.foodqual.2004.10.001
Go to original source...
- ROGINSKI, H., FUNGAY, J., FOX, P., 2003: Encyclopedia of Dairy Science, Vol. 1-4, London: Academic Press, p. 371-378. ISBN 0-12-227235-8.
- SADOWSKA, J., BIALOBRZEWSKI, I., JELINSKI, T., MARKOWSKI, M., 2009: Effect of fat content and storage time on the rheological properties of Dutch-type cheese. Journal of Food Engineering, 94, 3-4: 254-259. ISSN: 0260-8774. DOI: 10.1016/j.jfoodeng.2009.03.015
Go to original source...
- SHEEHAN, J. J., WILKINSON, M. G., MCSWEENEY, P. L. H., 2008: Influence of processing and ripening parameters on starter, non-starter and propionic acid bacteria and on the ripening characteristics of semi-hard cheeses. International Dairy Journal, 18, 9: 905-917. ISSN: 0958-6946. DOI: 10.1016/j.idairyj.2007.11.024
Go to original source...
- SMIT, G., SMIT, B. A., ENGELS, W. J. M., 2005: Flavour formation by lactic acid bacteria and biochemical flavour profilig of cheese products. FEMS Microbiology Reviews, 29, 3: 591-610. ISSN: 0168-6445. DOI: 10.1016/j.fmrre.2005.04.002
Go to original source...
- SNEDECOR, G. W., COCHRAN, W. G., 1967: Statistical Methods, 6th ed. Iowa: Iowa State University Press, 593 p. ISBN 0-8138-1560-6.
- SOUSA M. J., ARDO Y., McSWEENEY P. L. H., 2001: Advances in the study of proteolysis during cheese ripening. International Dairy Journal, 11, 4-7: 327-345. ISSN: 0958-6946. DOI: 10.1016/S0958-6946(01)00062-0
Go to original source...
- TOSO, B., PROCIDA, G., STEFANON, B., 2002: Determination of volatile compounds in cows milk using headspace GC-MS. Journal of Dairy Research, 69, 4: 569-577. ISSN: 0022-0299. DOI: 10.1017/S0022029902005782
Go to original source...
- VAN LEUVEN, I., VAN CAELENBERG, T., DIRINCK, P., 2008: Aroma characterisation of Gouda-type cheeses. International Dairy Journal, 18, 8: 790-800. ISSN: 0958-6946. DOI: 10.1016/j.idairyj.2008.01.001
Go to original source...
- VERZERA, A., ZIINO, M., CONDURSO, C., ROMEO, V., ZAPPALA, M., 2004: Solid-phase microextraction and gass chromatography-mass spectrometry for rapid characterisation of semi-hard cheese. Analytical and Bioanalytical Chemistry, 380, 7-8: 930-936. ISSN: 1618-2642. DOI: 10.1007/s00216-004-2879-4
Go to original source...
- VÍTOVÁ, E., LOUPANCOVÁ, B., ZEMANOVÁ, J., ŠTOUDKOVA, H., BŘEZINA, P., BABÁK, L., 2006: Solid-phase microextraction for analysis of mould cheese aroma. Czech Journal of Food Sciences, 24, 6: 268-274. ISSN: 1212-1800. DOI: 10.17221/3324-CJFS
Go to original source...
- VÍTOVÁ, E., LOUPANCOVÁ, B., ŠTOUDKOVÁ, H., ZEMANOVÁ, J., 2007: Application of SPME-GC method for analysis of the aroma of white surface mould cheeses. Journal of Food and Nutrition Research, 46, 2: 84-90. ISSN: 1336-8672.
- YATES, M. D., DRAKE, M. A., 2007: Texture properties of Gouda cheese. Journal of Sensory Studies, 22, 5: 493-506. ISSN: 0887-8250. DOI: 10.1111/j.1745-459X.2007.00124.x
Go to original source...
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